10.... 236.6 cm3 de-encapsulated legume meats (sieve size #10)
To a 2-L jacketed round reactor vessel (reactor #1) with an overall
heat-transfer coefficient of about 100 Btu/F-ft2-hr add one, two, and three
with constant agitation.
In a second 2-L reactor vessel with a radial flow impeller operating at 100
rpm add four, five, six, and seven until the mixture is homogeneous.
To reactor #2 add eight followed by three equal portions of the homogeneous
mixture in reactor #1. Additionally, add nine and ten slowly with constant
agitation. Care must be taken at this point in the reaction to control any
temperature rise that may be the result of an exothermic reaction.
Using a screw extrude attached to a #4 nodulizer place the mixture
piece-meal on a 316SS sheet (300 x 600 mm). Heat in a 460K oven for a
period of time that is in agreement with Frank & Johnston's first order
rate expression (see JACOS, 21, 55), or until golden brown.
Once the reaction is complete, place the sheet on a 25 deg. C heat-transfer
table allowing the product to come to equilibrium.